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GC/MS: A Valid Tool for Soil Gas Hydrocarbons Speciation

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DOI: 10.4236/ijamsc.2015.33007    3,101 Downloads   3,777 Views  

ABSTRACT

This work describes an alternative method based on GC/MS technique with SCAN-ion approach for speciation of hydrocarbons contained in soil gas matrices and sampled on solid sorbent tubes (coconut shell charcoal).

Conflicts of Interest

The authors declare no conflicts of interest.

Cite this paper

Clerici, L. , Mongini, E. , Robles, P. , Dellavedova, P. and Gregorio, M. (2015) GC/MS: A Valid Tool for Soil Gas Hydrocarbons Speciation. International Journal of Analytical Mass Spectrometry and Chromatography, 3, 54-62. doi: 10.4236/ijamsc.2015.33007.

References

[1] Mayer, C.L. (In Press) Guidance Document for Soil-Gas Surveying, Prepared under EPA EMSL-LV Contract n. 68033245. Lockheed Engineering and Sciences Company, Las Vegas.
[2] Cambiaghi, M., Cogliati, N. and Maspero, M. (2009) Idrocarburi e analisi di rischio: problemi e interpretazioni. Acqua & Aria, 5, 18-23.
[3] Department of Environmental Protection (2004) Method for the Determination of Volatile Petroleum Hydrocarbons (VPH), Revision 1.1. Department of Environmental Protection, Massachusetts
[4] Department of Environmental Protection (2004) Method for the Determination of Extractable Petroleum Hydrocarbons (EPH), Revision 1.1. Department of Environmental Protection, Massachusetts.
[5] Department of Environmental Protection (2009) Method for Determination of Air-Phase Petroleum Hydrocarbon (APH), Final Revision 1. Department of Environmental Protection, Massachusetts.
[6] EURACHEM (1998) The Fitness for Purpose of Analytical Methods—A Laboratory Guide to Method Validation and Related Topics. EURACHEM Guide, 22.
[7] UNI EN 13649-2002. Emissioni da sorgente fissa—Determinazione della concentrazione in massa di singoli composti organici in forma gassosa. Metodo mediante carboni attivi e desorbimento con solvente; §7 Procedimento analitico, §§ 7.1. Desorbimento del campione.
[8] EPA (1999) Compendium Method TO-15.
[9] EURACHEM-CITAC Guide (2011) Quantifying Uncertainty in Analytical Measurement, Third Edition.

  
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