Fabrication, Mechanical and Dielectric Characterization of 3D Orthogonal Woven Basalt Reinforced Thermoplastic Polyimide Composites

DOI: 10.4236/jtst.2015.11005   PDF   HTML   XML   4,702 Downloads   5,359 Views   Citations


The 3D orthogonal woven basalt fiber reinforced polyimide (PI) composites were fabricated and characterized in this study. The PI film was firstly prepared to determine PI processing parameters. Fourier transform infrared (FTIR) analysis showed that 300°C was the suitable imidization temperature. Thermal gravimetric analysis (TGA) and differential scanning calorimetry (DSC) results showed relatively good thermal properties of the PI film. In the fabrication of composites, the multi-step impregnation method was applied. The bending properties of 3 mm-thick composite showed increasing trend in all and the second-time impregnated composite had much higher value than the first-time impregnated composite. Moreover, the bending fracture mode photos showed obvious creases except for the first-time impregnated materials, which agreed well with the bending property values. The dielectric constants for the composites were complex because they had not regular value following the mixing rule of the composites, which was mainly due to the interfacial polarization and other effects in the fabrication processing.

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Hou, S. , Xie, J. , Kuang, Y. , Zheng, X. , Yao, L. and Qiu, Y. (2015) Fabrication, Mechanical and Dielectric Characterization of 3D Orthogonal Woven Basalt Reinforced Thermoplastic Polyimide Composites. Journal of Textile Science and Technology, 1, 35-44. doi: 10.4236/jtst.2015.11005.

Conflicts of Interest

The authors declare no conflicts of interest.


[1] Sheng, D., Wang, H., Ying, Z., Wang, H.T. and Ying, Z.H. (2013) Application of Thermoplastic Polyimide Composite in Aerospace Field. Plastics, 42, 46-48.
[2] Xu, H.Y., Yang, H.X., Tao, L.M., Liu, J.G., Fan, L. and Yang, S.Y. (2010) Preparation and Properties of Glass Cloth- Reinforced Meltable Thermoplastic Polyimide Composites for Microelectronic Packaging Substrates. High Performance Polymers, 22, 581-597. http://dx.doi.org/10.1177/0954008309354609
[3] Yu, L. and Cheng, X. (2013) Tensile Property of Surface-Treated Poly-p-phenylenebenzobisoxazole (PBO) Fiber-Reinforced Thermoplastic Polyimide Composite. Journal of Thermoplastic Composite Materials, 26, 307-321.
[4] Li, J. and Cheng, X.H. (2007) Effect of Rare Earth Solution on Mechanical and Tribological Properties of Carbon Fiber Reinforced Thermoplastic Polyimide Composite. Tribology Letters, 25, 207-214.
[5] Li, J. and Cheng, X.H. (2008) Evaluation of Tribological Performance of Surface-Treated Carbon Fiber-Reinforced Thermoplastic Polyimide Composite. Journal of Applied Polymer Science, 107, 1147-1153.
[6] Paplham, W.P., Seferis, J.C., Calleja, F.J.B. and Zachmann, H.G. (1995) Microhardness of Carbon-Fiber-Reinforced Epoxy and Thermoplastic Polyimide Composites. Polymer Composites, 16, 424-428.
[7] Rodeffer, C.D., Maybach, A.P. and Ogale, A.A. (1996) Influence of Thermal Aging on the Transverse Tensile Creep Response of a Carbon Fiber Thermoplastic Polyimide Composite. Journal of Advanced Materials, 27, 46-51.
[8] Pankow, M., Quabili, A. and Yen, C.-F. (2014) Hybrid Three-Dimensional (3-D) Woven Thick Composite Architectures in Bending. Journal of Materials Science, 66, 255-260.
[9] Sun, B., Zhang, R., Zhang, Q., Gideon, R. and Gu, B. (2013) Drop-Weight Impact Damage of Three-Dimensional Angle- Interlock Woven Composites. Journal of Composite Materials, 47, 2193-2209.
[10] Udatha, P., Kumar, C.V.S., Nair, N.S. and Naik, N.K. (2012) High Velocity Impact performance of Three-Dimensional Woven Composites. Journal of Strain Analysis for Engineering Design, 47, 419-431.
[11] Yao, L., Wang, X., Liang, F., Wu, R., Hu, B., Feng, Y., et al. (2008) Modeling and Experimental Verification of Dielectric Constants for Three-Dimensional Woven Composites. Composites Science and Technology, 68, 1794-1799.
[12] Callus, P.J., Mouritz, A.P., Bannister, M.K. and Leong, K.H. (1999) Tensile Properties and Failure Mechanisms of 3D Woven GRP Composites. Composites Part A: Applied Science and Manufacturing, 30, 1277-1287. http://dx.doi.org/10.1016/S1359-835X(99)00033-0
[13] Cox, B.N., Dadkhah, M.S. and Morris, W.L. (1996) On the Tensile Failure of 3D Woven Composites. Composites Part A: Applied Science and Manufacturing, 27, 447-458.
[14] Qiu, Y.P., Xu, W., Wang, Y.J., Zikry, M.A. and Mohamed, M.H. (2001) Fabrication and Characterization of Three- Dimensional Cellular-Matrix Composites Reinforced with Woven Carbon Fabric. Composites Science and Technology, 61, 2425-2435.
[15] Tan, P., Tong, L.Y., Steven, G.P. and Ishikawa, T. (2000) Behavior of 3D Orthogonal Woven CFRP Composites. Part I. Experimental Investigation. Composites Part A: Applied Science and Manufacturing, 31, 259-271. http://dx.doi.org/10.1016/S1359-835X(99)00070-6
[16] Czigany, T. (2005) Basalt Fiber Reinforced Hybrid Polymer Composites. Materials Science Forum, 473-474, 59-66. http://dx.doi.org/10.4028/www.scientific.net/MSF.473-474.59
[17] Subagia, I.D.G.A., Kim, Y., Tijing, L.D., Kim, C.S. and Shon, H.K. (2014) Effect of Stacking Sequence on the Flexural Properties of Hybrid Composites Reinforced with Carbon and Basalt Fibers. Composites Part B: Engineering, 58, 251-258.
[18] Wang, J., Chen, B., Liu, N., Han, G. and Yan, F. (2014) Combined Effects of Fiber/Matrix Interface and Water Absorption on the Tribological Behaviors of Water-Lubricated Polytetrafluoroethylene-Based Composites Reinforced with Carbon and Basalt Fibers. Composites Part A: Applied Science and Manufacturing, 59, 85-92.
[19] Yao, L., Li, W.B., Wang, N., Li, W., Guo, X. and Qiu, Y.P. (2007) Tensile, Impact and Dielectric Properties of Three Dimensional Orthogonal Aramid/Glass Fiber Hybrid Composites. Journal of Materials Science, 42, 6494-6500.

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