Optimization of Dry Ashing of Whole Blood Samples for Trace Metal Analysis

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DOI: 10.4236/ajac.2011.28114    6,215 Downloads   11,288 Views  Citations

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ABSTRACT

Dry ashing is an established method. Ashing whole blood samples are, however, often difficult to carry out with significant sample loss, and the procedure is not well documented. A new procedure has been devel- oped and optimized to dry-ash whole blood samples for trace metal analyses. The procedure reduces both the dry-ashing time by more than two thirds and sample loss. The ashed sample can be readily used in subse- quent, simultaneous or individual analysis of several metals by ICP-OES, as demonstrated in the analysis of a whole blood sample. The new procedure is simple, inexpensive, and faster than the established method.

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S. Bragg and Z. Xue, "Optimization of Dry Ashing of Whole Blood Samples for Trace Metal Analysis," American Journal of Analytical Chemistry, Vol. 2 No. 8, 2011, pp. 979-983. doi: 10.4236/ajac.2011.28114.

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