The Synthesis of Solvent-Free TiO2 Nanofluids through Surface Modification

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DOI: 10.4236/snl.2011.12008    5,885 Downloads   12,050 Views  Citations

ABSTRACT

TiO2 nanoparticles with surface hydroxyl groups are treated by trimethoxysilane (CH3O)3Si(CH2)3O(CH2CH2O)6-9CH3 and a inorganic core/organic shell hybridmaterials, which shows itself a yellow viscous fluid, is obtained. We call it solvent-free TiO2 nanofliuds. Transmission electron microscopy (TEM), Fourier transform infrared spectrum (FTIR), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and rheometer are adopted to characterize the product. As a result, the content of TiO2 nanoparticles in the nanofliuds is about 5.5wt%, the functionalized TiO2 nanoparticles possess better dispersion, very low viscosity and an obvious liquid-like behavior at room temperature in absence of solvent.

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Yu, P. , Zheng, Y. and Lan, L. (2011) The Synthesis of Solvent-Free TiO2 Nanofluids through Surface Modification. Soft Nanoscience Letters, 1, 46-50. doi: 10.4236/snl.2011.12008.

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