Structural and microstructural characteristics of B-doped PbTe semiconductor

Abstract

The main task of this paper was accurate determination of structural and microstructural parameters of B-doped PbTe semiconductor (“p” type). Four samples (undoped PbTe, and three doped with initial B contents: 1 %, 3 % and 8 %) were synthesized using the Bridgman method and analysed using X-ray powder diffraction (XRD) technique. Structural features were obtained using the Rietveld method and microstructural by diffraction-line broadening methods. Microstructural measurements contain both crystallite domain sizes and microstrain calculations obtained by the Warren-Averbach and the simplified integral-breadth methods.

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J. Stojanovic, "Structural and microstructural characteristics of B-doped PbTe semiconductor," Journal of Minerals and Materials Characterization and Engineering, Vol. 5 No. 2, 2006, pp. 143-153. doi: 10.4236/jmmce.2006.52010.

Conflicts of Interest

The authors declare no conflicts of interest.

References

[1] BALZAR, D., LEDBETTER, H., 1997, “Software for comparative analysis of diffraction – line boadening.” Advances in X – ray analysis, vol. 39, edited by V. Gilfrich et al., Plenum Press, New York, pp. 457 – 464.
[2] RODRIGUEZ – CARVAJAL, J., 1995, “User’s guide to program FULLPROF.” 2004-LLBJRC (Laboratorie León Brillouin, CEA-CNRS, Centre d’Etudes de Saclay, Gif sur Yvette, France).
[3] YASUTOSHI, N., SHIGERU, O., SHOISHI, S. & YOSHIHIKO, S., 1983, “Charge distribution and atomic thermal vibrations in lead chalcogenide crystals.” Acta Cryst., B39, pp. 312 – 317.
[4] YASUTOSHI, N., KATASHI, M., SHOISHI, S., YOSHIHIKO, S., KOSHIRO, T & IWAO, I. 1987, “Temperature dependence of atomic thermal parameters of lead chalcogenides, PbS, PbSe, PbTe.” Acta Cryst., C43, pp. 1443 – 1445.

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